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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 2
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Original Articles

Samarium Mediated Reductive Coupling Cyclization of α-Phenylsulfonylcinnamonitriles Catalyzed by Viologen Under Room Temperature Conditions

Xingliang Zheng Department of Chemistry, Zhejiang University, Xixi Campus, 148 Tian Mu Shan Road, Hangzhou, 310028, P.R. China
&
Yongmin Zhang Department of Chemistry, Zhejiang University, Xixi Campus, 148 Tian Mu Shan Road, Hangzhou, 310028, P.R. China; State Key Laboratory of Organometallic Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai, P.R. ChinaCorrespondence[email protected]
Pages 265-273 | Received 12 May 2003, Published online: 18 Oct 2011
 
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Abstract

Promoted by metallic samarium and catalyzed by viologen, the intermolecular reductive coupling cyclization reactions of α-phenylsulfonylcinnamonitriles were studied. A possible reaction mechanism was proposed.

Acknowledgments

We are grateful to the National Natural Science Foundation of China (Project No.20072033) and the Specialized Research Fund for the Doctoral Program of Higher Education for financial support.

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