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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 7
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Original Articles

Allyltriphenylphosphonium Peroxodisulfate (CH2˭CHCH2PPh3)2S2O8: An Efficient and Convenient Reagent for the Oxidation of Alcohols and Silyl and THP‐Ethers Under Nonaqueous Conditions

M. Tajbakhsh Department of Chemistry, Faculty of Science, University of Mazandaran, Babolsar, 47415, IranCorrespondence[email protected]
,
M. M. Lakouraj Department of Chemistry, Faculty of Science, University of Mazandaran, Babolsar, 47415, IranCorrespondence[email protected]
&
A. Fadavi Department of Chemistry, Faculty of Science, University of Mazandaran, Babolsar, 47415, Iran
Pages 1173-1181 | Received 22 Apr 2003, Published online: 21 Aug 2006
 
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Abstract

The preparation of allyltriphenylphosphonium peroxodisulfate (ATPPD) as a new and efficient reagent for the oxidation of primary and secondary alcohols, trimethylsilyl and tetrahydropyranyl (THP) ethers to their corresponding carbonyl compounds in refluxing acetonitrile with 1.1:1 molar equivalents of the oxidant is described.

Acknowledgment

We are thankful to the Mazandaran University for the partial support of this work.

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