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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 8
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Original Articles

Synthesis of γ‐Substituted‐β‐(Ethoxycarbonyl)allylsilanes via Peterson Olefination

Hideyuki Suzuki Department of Chemistry, Rikkyo University, Nishi‐Ikebukuro, Toshima‐ku, Tokyo, 171‐8501, Japan
,
Soichi Ohta Department of Chemistry, Rikkyo University, Nishi‐Ikebukuro, Toshima‐ku, Tokyo, 171‐8501, Japan
&
Chiaki Kuroda Department of Chemistry, Rikkyo University, Nishi‐Ikebukuro, Toshima‐ku, Tokyo, 171‐8501, JapanCorrespondence[email protected]
Pages 1383-1392 | Received 06 Oct 2003, Published online: 21 Aug 2006
 
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Abstract

γ‐Substituted‐β‐(ethoxycarbonyl)allylsilanes were synthesized via a Peterson olefination using ethyl 2,3‐bistrimethylsilylpropanoate.

Acknowledgment

The authors must thank Dr. A. Ishiwata of the Institute of Physical and Chemical Research for the measurement of high‐resolution mass spectra. Thanks are also due to Prof. E. Horn of Rikkyo University for help in the writing of this article.

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