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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 11
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Original Articles

Solid Supported Microwave‐Assisted Beckmann Rearrangement of Ketoximes in Dry Media

Firouz Matloubi Moghaddam Department of Chemistry, Sharif University of Technology, P.O. Box 11365‐9516, Tehran, IranCorrespondence[email protected]
,
Abbas Ali Rastegar Rad Department of Chemistry, Sharif University of Technology, P.O. Box 11365‐9516, Tehran, Iran
&
Hassan Zali‐Boinee Department of Chemistry, Sharif University of Technology, P.O. Box 11365‐9516, Tehran, Iran
Pages 2071-2075 | Received 10 Dec 2003, Published online: 20 Aug 2006
 
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Abstract

An AlCl3–ZnCl2 mixture supported on silica gel is found to be a new efficient medium for the Beckmann rearrangement in solvent‐free conditions under microwave irradiation. The yields are good to excellent.

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