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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 13
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Original Articles

Facile Synthesis of Aminoalcohols by Ring Opening of Epoxides Under Solvent Free Conditions

Gloria Huerta Instituto de Química‐UNAM, Circuito Exterior, Ciudad Universitaria, Coyoacán, C. P. 04510, México, DF, México
,
Guadalupe Contreras‐Ordoñez Instituto de Química‐UNAM, Circuito Exterior, Ciudad Universitaria, Coyoacán, C. P. 04510, México, DF, México
,
C. Alvarez‐Toledano Instituto de Química‐UNAM, Circuito Exterior, Ciudad Universitaria, Coyoacán, C. P. 04510, México, DF, México
,
Víctor Santes Instituto Mexicano del Petróleo, Programa de Tratamiento de Crudo Maya, Col. San Bartolo Atepehuacan, México, DF, México
,
Elizabeth Gómez Instituto de Química‐UNAM, Circuito Exterior, Ciudad Universitaria, Coyoacán, C. P. 04510, México, DF, MéxicoCorrespondence[email protected]
&
Rubén A. Toscano Instituto de Química‐UNAM, Circuito Exterior, Ciudad Universitaria, Coyoacán, C. P. 04510, México, DF, México
Pages 2393-2406 | Received 02 Mar 2004, Published online: 10 Jan 2011
 
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Abstract

The convenient cleavage of symmetrical and unsymmetrical epoxides with either aromatic or aliphatic amine under solvent free conditions is reported. The reactions were carried out in a sealed ampoule at 90°C to give regioselectively the corresponding β‐amino alcohol in one pot in high yields.

Acknowledgments

Financial support from DGAPA (IN 207103) is grateful acknowledged. Authors thank Francisco Javier Pérez, Luis Velasco, Myrian Adaya and Rocío Patiño for technical support.

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