Publication Cover
Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 43, 2013 - Issue 10
449
Views
2
CrossRef citations to date
0
Altmetric
Original Articles

Organic Preparations with Molar Amounts of Volatile Malodorous Thiols

, &
Pages 1447-1454 | Received 06 Sep 2011, Published online: 05 Mar 2013

REFERENCES

  • For Germany: DVGW Rules, Gas odorisation Technical rule worksheet G 280-1, August 2004 .
  • Fanghänel , E. ; Alsleben , I. ; Gebler , B. ; Herrmann , A. ; Herrmann , R. ; Palmer , T. ; Strunk , K. ; Ullrich , A. ; Lüders , K. ; Mahdjour , H. Chemistry of multisulfur substituted arenes and sulfur-rich heterocycles—relations to advanced materials . Phosphorus, Sulfur Silicon Relat. Elem. 1997 , 120 , 121 – 143 .
  • Testaferri , L. ; Tiecco , M. ; Tingoli , M. ; Chianelli , D. ; Montanucci , M. Simple syntheses of aryl alkyl thioethers and of aromatic thiols from unactivated aryl halides and efficient methods for selective dealkylation of aryl alkyl ethers and thioethers . Synthesis. 1983 , 751 – 755 .
  • Becher , J. ; Stidsen , C. ; Toftlund , H. ; Asaad , F. Sodium 2-methyl-2-propylthiolate, a versatile sulfur reagent: Preparation of protected polysulfur ligands and their nickel(II) complexes . Inorg. Chim. Acta. 1986 , 121 , 23 – 26 .
  • Gingras , M. ; Raimundo , J. ; Chabre , Y. Persulfurierte aromatische Verbindungen . Angew. Chem. 2006 , 118 , 1718 – 1745 .
  • Sweetman , B. ; Vestling , M. ; Ticaric , S. ; Kelly , P. ; Field , L. ; Merryman , P. ; Jaffe , I. Biologically oriented organic sulfur chemistry, 8: Structure–activity relationships of penicillamine analogs and derivatives . J. Med. Chem. 1971 , 14 , 868 .
  • Fanghänel , E. ; Herrmann , R. ; Naarmann , H. Novel benzo [d] 1,2,3-trithioles and their hexachloroantimonates derived from benzenehexathiol . Tetrahedron. 1995 , 51 , 2533 – 2542 .
  • Yip , H. ; Schier , A. ; Riede , J. ; Schmidbaur , H. Benzenehexathiol as a template rim for a golden wheel: Synthesis and structure of [{CSAu (PPh 3)} 6] . J. Chem. Soc., Dalton Trans. 1994 , 1994 , 2333 – 2334 .
  • Fanghänel , E. ; Wegner , R. ; Beye , N. ; Peters , K. ; Müllen , K. Peralkylthio substituierte Dibenzotetrathiafulvalene (DBTTF) aus Benzolhexathiolat . J. Prakt. Chem. 1995 , 337 , 299 – 306 .
  • Testaferri , L. ; Tingoli , M. ; Tiecco , M. Reactions of polychlorobenzenes with alkanethiol anions in HMPA: A simple, high-yield synthesis of poly (alkylthio) benzenes . J. Org. Chem. 1980 , 45 , 4376 – 4380 .
  • MacNicol , D. ; Mallison , P. ; Murphy , A. ; Sym , G. An efficient synthesis of hexa-substituted benzenes and the discovery of a novel host conformation for hexakis ([β]-naphthylthio) benzene . Tetrahedron Lett. 1982 , 23 , 4131 – 4134 .
  • Gomberg , M. An instance of trivalent carbon: Triphenylmethyl. J. Am. Chem. Soc. 1900, 22, 757–771.
  • Takeshita , K. ; Ozawa , T. Recent progress in in vivo ESR spectroscopy . J. Radiation Res. 2004 , 45 , 373 – 384 .
  • Mäder , K. Pharmaceutical applications of in vivo EPR . Physics Med. Biol. 1998 , 43 , 1931 – 1935 .
  • Lurie , D. ; Mäder , K. Monitoring drug delivery processes by EPR and related techniques—Principles and applications . Adv. Drug Deliv. Rev. 2005 , 57 , 1171 – 1190 .
  • Liu , Y. ; Villamena , F. ; Sun , J. ; Xu , Y. ; Dhimitruka , I. ; Zweier , J. Synthesis and characterization of ester-derivatized tetrathiatriarylmethyl radicals as intracellular oxygen probes . J. Org. Chem. 2008 , 73 , 1490 – 1497 .
  • Bobko , A. ; Dhimitruka , I. ; Eubank , T. ; Marsh , C. ; Zweier , J. ; Khramtsov , V. Trityl-based EPR probe with enhanced sensitivity to oxygen . Free Radical Biol. Med. 2009 , 47 , 654 – 658 .
  • Bobko , A. ; Dhimitruka , I. ; Zweier , J. ; Khramtsov , V. Trityl radicals as persistent dual function pH and oxygen probes for in vivo electron paramagnetic resonance spectroscopy and imaging: concept and experiment . J. Am. Chem. Soc. 2007 , 129 , 7240 – 7241 .
  • Odorisio , P. ; Pastor , S. ; Spivack , J. ; Rodebaugh , R. 1,2,4,5-Tetramercaptobenezene: A facile route to the benzo[1,2-d:4,5-d']bis[1,3]dithiole ring system . Phosphorus, Sulfur Silicon Relat. Elem. 1982 , 13 , 309 – 313 .
  • Dirk , C. ; Cox , S. ; Wellman , D. ; Wudl , F. Isolation and purification of benzene-1,2,4,5-tetrathiol . J. Org. Chem. 1985 , 50 , 2395 – 2397 .
  • Tkachenko , B. ; Fokina , N. ; Chernish , L. ; Dahl , J. ; Liu , S. ; Carlson , R. ; Fokin , A. ; Schreiner , P. Functionalized nanodiamonds part 3: Thiolation of tertiary/bridgehead alcohols . Org. Lett. 2006 , 8 , 1767 – 1770 .
  • Lee , D. F. ; Saville , B. ; Trego , B. R. A simple synthesis of tertiary alkanethiols . Chem. Ind. (London). 1960 , 868 – 869 .
  • Pattenden , G. ; Shuker , A. , J. Synthetic approaches towards the novel 1,3-dioxo-1,2-dithiolane moiety in the antitumour antibiotic substance leinamycin . J. Chem. Soc., Perkin Trans. 1. 1992 , 10 , 1215 – 1221 .
  • Personal communications by several research group leaders in Germany and the US .
  • “Geruchs-Immissions-Richtlinie des Umweltbundesamtes.” Availables at http://www.umwelt-online.de/recht/luft/laender/girl_08_ges.htm
  • VDI/DIN-Handbuch Reinhaltung der Luft, Band 5: Analysen- und Messverfahren; VDI: Duesseldorf, Germany, 2449 .
  • Rheinboldf , H. ; Mott , F. ; Motzkus , E. Tertiäres Butylmercaptan . J. Prakt. Chem. (Leipzig). 1932 , 134 , 257 – 281 .
  • For Germany, TA Luft; BImschG; BImschV; DIN EN 12753. Accessible through Beuth Verlag GmbH, Am DIN-Platz, Berlin, Germany, http://www.beuth.de .
  • In Germany, this is required by DIN EN 12753. Accessible through Beuth Verlag GmbH, Am DIN-Platz, Berlin, Germany, http://www.beuth.de .
  • Dhimitruka , I. ; Velayutham , M. ; Bobko , A. ; Khramtsov , V. ; Villamena , F. ; Hadad , C. ; Zweier , J. Large-scale synthesis of a persistent trityl radical for use in biomedical EPR applications and imaging . Bioorg. Med. Chem. Lett. 2007 , 17 , 6801 – 6805 .
  • Pastor , S. ; Hessell , E. Substitution of unactivated aryl halides by thiolate anions in polyglymes . J. Org. Chem. 1985 , 50 , 4812 – 4815 .

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.