References
- To whom correspondence should be addressed
- Sandler , S. R. and Karo , W. 1968 . Organic Functional Group Preparations , Vol. I , 269 – 300 . New York, N.Y. : Academic Press . C. A. Buehler and D. E. Pearson, “Survey of Organic Syntheses,” pp. 894–936, Wiley-Interscience, New York, N.Y., 1970
- Walsh , E. N. and Toy , A. D. F. 1963 . Inorg. Synth. , 7 : 69
- Details of the mechanism remain to be determined
- When a lesser quantity of DMPADC was used, varying amounts of carboxylic anhydrides were obtained. If desired, the excess reagent can be recovered by distillation prior to the work-up of the reaction mixture
- This compound, bp 101°C/12 torr, was prepared from diethylamine and phosphorus oxychloride in a manner analogous to the preparation of DMPADC3