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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 11, 1981 - Issue 4
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Original Articles

Improved Syntheses of Nε-Tert-butyloxycarbonyl-L-lysine and Nα-Benzyloxycarbonyl-Nε-tert-butyloxycarbonyl-I-lysine

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Pages 303-314 | Published online: 05 Dec 2006

References

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  • Kappeler , H. and Schwyzer , R. 1961 . Helv. Chim. Acta , 44 : 1136
  • Felix , A. M. , Jimenez , M. H. , Mowles , T. and Meienhofer , J. 1978 . Int. J. Peptide Protein Res. , 11 : 329
  • Felix , A. M. , Jimenez , M. H. , Wang , C.-T. and Meienhofer , J. 1980 . ibid. , 15 : 342
  • Chang , C.-D. , Felix , A. M. , Jimenez , M. H. and Meienhofer , J. 1980 . ibid. , 15 : 485
  • Tzougraki , C. , Makofske , R. C. , Gabriel , T. F. , Michalewsky , J. , Meienhofer , J. and Li , C. H. 1980 . ibid. , 15 : 377
  • Bezas , B. and Zervas , L. 1961 . J. Am. Chem. Soc. , 83 : 719
  • Zervas , L. and Hamalidis , C. 1965 . ibid. , 87 : 99
  • Schwyzer , R. and Rittel , W. 1961 . Helv. Chim. Acta , 44 : 161
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  • Benoiton , L. 1966 . Biochemical Preparations , 11 : 80
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  • Scott , J. W. and Parker , D. 1980 . Org. Prep. Proc. Int. , 12 : 242
  • Ragnarsson , U. , Karlsson , S. M. , Sandberg , B. E. and Larsson , L. E. 1973 . Org. Syn. , 53 : 25
  • Moroder , L. , Hallett , A. , Wünsch , E. , Keller , O. and Wersin , G. 1976 . Z. Physiol. Chem. , 357 : 1651
  • Barral , I. and Savrda , J. 1973 . Synthesis , : 759
  • If the solution is allowed to stand, the copper complex 2 may precipitate
  • 1978 . Separating Metals Using Chelex 100 Chelating Resin The resin should be stored in its acid form for as short a time as possible. The resin handling methods are adapted from Bio-Rad Laboratories, Product Information 2020, (July
  • Any of the less soluble Nϵ-benzyloxycarbonyl-L-lysine formed will precipitate at this point and can be removed by filtration;11 in our runs, we observed none of this material

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