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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 13, 1983 - Issue 12
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Original Articles

A Facile Preparation of Aliphatic Hydroxamic Acid from N,N,O-Tris(Trimethylsilyl)Hydroxylamine and Acid Chloride

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Pages 1053-1056 | Published online: 06 Feb 2007

References

  • Bauer , L. and Exner , O. 1974 . Angew. Chem. Int. Ed. Engle. , 13 : 376
  • Sosnovsky , G. and Krogh , J. 1980 . Synthesis , : 654
  • Yamada , K. , Kanekiyo , T. , Tanaka , S. , Naruchi , K. and Yamamoto , M. 1981 . J. Am. Chem. Soc , 103 : 7003
  • Wannagat , U. and Smrekar , O. 1969 . Monatshefte fur Chemie , 100 : 750 See also: King, F.D. and Walton, D.R.M., Synthesis, 1975, 788 N,N,O-Tris(trimethylsilyl)hydroxylamine was prepared from N,O-bis(trimethylsilyl)hydroxylamine with nBuLi followed by treatment with trimethylchlorosilane according to the procedure described by Wannagat et al:
  • 1920 . Beilstains Handbuch der Organischen Chemie Vol. II , II, 1st supplement (1929): II, 2nd supplement (1942).
  • Kornblum , N. and Brown , R. A. 1965 . J, Am. Chem. Soc , 87 : 1742
  • Fishbein , W. N. , Darley , J. and Streeter , C. L. 1965 . Anal, Biochem. , 28 : 13
  • Jones , L. W. and Neuffer , L. 1929 . J. Am. Chem. Soc , 39 : 659
  • 1941 . Chemical Abstracts , 35 : 730 Yields are not shown
  • Jones , L. W. and Hurd , C. D. 1921 . J. Am. Chem. Soc , 43 : 2422
  • Org. Synth. Coll. , Vol. II. 67

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