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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 16, 1986 - Issue 4
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Original Articles

An Efficient Preparation of Alkyl α-Bromomethylacrylates by Dehydrobromination of Alkyl β,β′-Dibromoisobutyrates with Potassium Fluoride

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Pages 387-392 | Published online: 05 Dec 2006

References

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  • Anhydrous ‘Gold Label’ potassium fluoride from the Aldrich Chemical Co., Milwaukee, WI, was powdered (mortar and pestle) and used without further drying. Any other samples of potassium fluoride that were used were first powdered and then dried at 50°C (1.0 mm) in a drying pistol over P2O5

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