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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 17, 1987 - Issue 13
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Original Articles

Polymer-Supported Phosphine-Halogen Complexes 41. Improved Formylation of Alcohols with Dimethylformamide

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Pages 1629-1636 | Published online: 06 Dec 2006

References

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  • IR (CHC13): 1705 cm–1; 1H NMR (CC14): 8.10 (s, 1H, H–C=0), 4.60 (t, 1H, J=6 Hz, H–C–CHO) ppm
  • IR (CHC1): 1700 cm–1; 1H NMR (CC14): 8.10 (s, 1H, H–C=0), 4.80 (m, 1H, H–C–CHO) ppm
  • IR (CHC1): 1710 cm–1; 1H NMR (CC14): 8.10 (s, 1H, H–C=0), 4.15 (t, 1H, J=6 Hz, H–C–CHO) ppm
  • IR (CHC1): 1720 cm–1; 1H NMR (CC14): 8.11 (s, 1H, H–C=0), 5.37 (bs, W1/2=6 Hz, 1H, H–C–CHO), 1.54 (3H), 1.43 (3H), 1.33 (6H) (3s, isopropyliden CH3) ppm

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