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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 19, 1989 - Issue 11-12
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Original Articles

An Improved Synthesis of A Chemiluminescent Cyclic Hydrazide: N-(7-Aminobutyl)-N-Ethyl-Naphthalene-1,2-Dicarboxylic Hydrazide

Clifford M. Chan Diagnostics Division, Abbott laboratories, Abbott Park, North Chicago II, 60064
Pages 1981-1985 | Received 27 Jan 1989, Published online: 24 Oct 2006

References

  • Gore , M. J. 1985 . Clincial Chemistry New , 11 : 1
  • Roswell , D. F. and White , E. H. 1978 . Methods in Enzymology , Vol. LVII , 409 Academic Press .
  • Gundermann , K. D. , Horstmann , W. and Bergmann , G. 1965 . Justus Liebigs Ann. Chem. , 127 : 684
  • Diment , J. A. 1968,1972 . Aust. J. Chemistry , : 22
  • 4-Nitrostyrene was purchased from Fairfield Chem. Co., Blythewood, South Carolina.
  • A: NMR (CDCl3) : 3.87 (s, 3H), 4.0 (s, 3H). Mass Spec. m/e: 289[M], 258[M -OCH3).
  • B: NMR (CDCl3) : 3.9 (s, 3H), 4.0 (s,3H). Mass Spec. m/e: 259[M], 248[M -OCH3).
  • C: NMR (CDCl3) : 1.7 (m, 4H), 3.9 (s, 3H), 4.0 (s,3H). Mass Spec. m/e: 460[M], 429[M -OCH3).
  • D: NMR (CDCl3) : 3.9 (s, 3H), 4.05 (s,3H). Mass Spec. m/e: 488[M], 457[M -OCH3).
  • E: NMR (CDCl3) : 1.2(m,3H), 1.5 (m,4H). Mass Spec. m/e: 326[M].

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