References
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- Hope , E. G. , Kemmitt , T. and Levason , W. 1988 . Organometallics , 7 : 78 197 – 198 . See also ref. 5
- This solution must be clear or only slightly turbid, indicating the absence of the (unsoluble) 1:1 complex t-BuOK-t-BuOH
- Gilman , H. and Gaj , B. J. 1957 . J. Org. Chem. , 22 : 1165 The excess of BuLi-t-BuOK reagent reacts with THF to give ethene and H2C[dbnd]CHOK, which does not interfere in the reaction with the electrophiles or chalcogenes. Compare:
- Quenching of this mixture with Me3SiCl, gave 3 in yields higher than 80%. See ref. 1