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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 20, 1990 - Issue 1
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Original Articles

Rapid Synthesis of α,β Unsaturated Iodides: Iodination Under Vacuum with Solid Diphosphorus Tetraiodide

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Pages 41-44 | Received 28 Jul 1989, Published online: 24 Oct 2006

References

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  • 4c: RMN: 1H (400 MHz) (CCl4) δ (/TMS): 1.90 (s, 6H), 2.16 (m, 2H) 3.29 (m, 2H); 13C (20.15 MHz) (CDCl3) δ (/TMS): 1.64 (CH2I), 37.66(CH3), 49.18 (CI), 54.71 (CH2); MS (70 ev) (M+ -I): 196.98202 (Calc.: 196.9828)
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