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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 20, 1990 - Issue 1
72
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Original Articles

A New Procedure to Δ4-3-Ketosteroids from 5β-3-Ketosteroids

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Pages 131-136 | Received 15 Aug 1989, Published online: 24 Oct 2006

References

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  • Crude isolated yield based on starting ketone: CrO3/2 Py: 65–86%
  • CrO3/AcOH: 25–60%
  • PCC: 5–10%
  • All Compounds reported herein have mp and spectral data consistent with the assigned structures. We thank Dr. K. Fisher from Lousiana State University for recording the mass spectra

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