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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 20, 1990 - Issue 4
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Original Articles

Temperature Dependent Addition Reactions During Photolysis of Aryl Vinyl Sulfides and Aryl Vinyl Ethers. Design and Construction of a Variable Temperature Photoreactor

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Pages 541-547 | Received 16 Oct 1989, Published online: 24 Oct 2006

References

  • Dittami , J. P. , Ramanathan , H. and Breining , S. 1989 . Tet. Lett. , 30 : 795
  • All photochemical experiments were conducted using a 450‐watt Canrad‐Hanovia medium pressure quartz mercury‐vapor lamp. The lamp was placed in a water cooled and vacuum jacketed quartz immersion well fitted with a pyrex sleeve filter. Reaction solutions were saturated with argon prior to irradiation
  • Vineland, New Jersey : Ace Glass Inc. . Available from, 08360
  • Waltham, Mass : G. Finkenbeiner Inc. . The photochemical apparatus described herein was constructed by, 33 Rumford Ave., 02154
  • Vineland, New Jersey : Ace Glass Inc. . Absorption sleeves are available in a variety of wavelength ranges from, 08360
  • Owsley , D. C. and Bloomfield , J. J. 1971 . Org. Prep Proc. Int. , 3 : 61 For another example of a photochemical reactor which relies on triple wall construction for low temperature operation see:, and Owsley, D.C. and Bloomfield, Org. Photochem. Synth., 1976, 2, 36
  • Newington, New Hampshire : Neslab Instruments, Inc. . 25 Nimble Hill Road, 03801
  • Temperature measurements were made using an Omega Digital Thermometer (Model No. 2175A) with a Type J Iron/Constantan thermocouple. The system was allowed to reach thermal equilibrium prior to turning on the lamp

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