Publication Cover
Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 21, 1991 - Issue 8-9
88
Views
13
CrossRef citations to date
0
Altmetric
Original Articles

Synthesis and 125Te NMR Spectroscopy of α-Tellurocarbonyl Compounds and Derivatives

, &
Pages 1105-1119 | Received 18 Mar 1991, Published online: 23 Sep 2006

References

  • Eisenberg , F. 1966 . “The Chemistry of the Carbonyl Group,” , Edited by: Patai , S. 331 – 370 . John Wiley and Sons . chap. 7
  • Luthra , N. P. and Odom , J. D. 1986 . “The Chemistry of Organic Selenium and Tellurium Compounds,” , Edited by: Patai , S. and Rappoport , A. Vol. 1 , 189 – 241 . New York : John Wiley and Sons . chap 6
  • Harris , R. K. and Mann , B. E. , eds. 1978 . “NMR and the Periodic Table,” , 412 – 415 . Academic Press . chap 12
  • Stefani , H. A. , Comasseto , J. V. and Petragnani , N. 1987 . Synthetic Commun. , 17 : 443
  • Huang , X. , Yuqing , H. and Huang , Z. 1989 . Synthetic Commun. , 19 : 1625
  • Engman , L. 1986 . Organometallics , 5 : 427
  • Engman , L. and Cava , M. P. 1982 . J. Org. Chem. , 47 : 3946
  • Ramasamy , K. , Kalyanasundarani , S. K. and Shammugan , P. 1978 . Synthesis , : 311
  • Clive , D. L. J. and Menchen , S. M. 1980 . J. Org. Chem. , 45 : 2347
  • Clive , D. L. J. and Beaulieu , P. L. 1982 . J. Org. Chem. , 47 : 1124
  • Kambe , N. , Inagaki , T. , Miyoshi , N. , Ogawa , A. and Sonoda , N. 1987 . Chem. Lett. , : 1171
  • Barton , D. H. R. , Bohe , L. and Lusinchi , X. 1988 . Tetrahedron Lett. , 29 : 2571
  • Petragnani , N. and Comasseto , J. V. 1986 . Synthesis , : 1
  • Engaman , L. and Cava , M. P. 1982 . J. Org. Chem. , 47 : 3946
  • Barton , D. H. R. and McCombie , S. W. J. 1975 . J. Chem. Soc., Perkin Trans. 1 , : 1574
  • Hashimoto , S. , Sakata , S. , Sonegawa , M. and Ikegami , S. 1988 . J. Am. Chem. Soc. , 110 : 3670
  • Use of α-chloroesters and ketones gave primarily reduction of the carbon-chlorine bond.
  • Osuka , A. and Suzuki , H. 1983 . Chem. Lett. , : 119
  • Discordia , R. P. and Dittmer , D. C. 1988 . Tetrahedron Lett. , 29 : 4929
  • Polson , G. and Dittmer , D. C. 1988 . J. Org. Chem. , 53 : 791
  • Zefirov , N. S. and Makhon'kov , D. I. 1982 . Chem. Rev. , 82 : 615
  • Hiiro , T. , Kambe , N. , Ogawa , A. , Noritaka , M. , Murai , S. and Sonoda , N. 1987 . Synthesis , : 1096
  • The product was found to be unstable with decomposition taking place in minutes in ethereal or hydrocarbon solvents; however, it was stable in methylene chloride at -20 °C for months. Overll stability could be increased by working up and storing the tellurides in halogenated sovlents, under nitrogen. It was eventually found that silica gel chromatography could be routinely performed using CH2Cl2/hexanes soulution as the eluent
  • Negishi , E. 1980 . “Organometallics in Organic Synthesis,” , Vol. 1 , New York : John Wiley and Sons .
  • Luthra , N. P. , Boccanfuso , A. M. , Dunlap , R. B. and Odom , J. D. 1988 . J. Organometal. Chem. , 354 : 51
  • Iriarte , J. M. , Silks , L. A. and Odom , J. D. 1988 . Southeastern Regional American Chemical Society Meeting . Nov. 1988 , Atlanta, Ga.. Inorganic Section, Abstr. No. 415
  • Kofron , W. G. and Baclawski , L. M. 1976 . J. Org. Chem. , 41 : 1879

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.