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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 22, 1992 - Issue 19
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Original Articles

A New Route to Synthesize 2,9-Dicarbonitrile-1,10-phenanthroline

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Pages 2811-2814 | Received 21 May 1992, Published online: 23 Sep 2006

References

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  • Sjögren , M. , Hansson , S. , Norrby , P-O. , Åkermark , B. , Cucciolito , M. E. and Vitagliano , A. 1992 . J. Amer. Chem. Soc. , (in press). to be published
  • Chandler , C. J. , Deady , L. W. and Reiss , J. A. 1981 . J. Heterocyclic Chem. , 18 : 599
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  • Lüning , U. and Müller , M. 1989 . Liebigs Ann. Chem. , : 367
  • Seyhan , M. and Fernelius , W. C. 1958 . Chem. Ber. , 91 : 469 An earlier report on this oxidation gave the unsymmetrical compound 2-formyl-9-carboxy-1,10-phenanthroline as the product
  • Newkome , G. R. , Kiefer , G. E. , Puckett , W. E. and Vreeland , T. 1983 . J. Org. Chem. , 48 : 5112
  • Mowry , D. T. and Butler , J. M. 1963 . Org. Synth. Coll. , 4 : 486
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  • Because of the poor solubility of the diamide, it was necessary to heat the mixture. The solution was allowed to cool until it just begun to become cloudy. It was then added to the rection mixture

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