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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 22, 1992 - Issue 3
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Original Articles

E-1-Lithio-1-Alkenes in Hydrocarbon Solvent

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Pages 477-480 | Accepted 05 Sep 1991, Published online: 05 Dec 2006

References

  • Polt , R. and Peterson , M. A. 1990 . Tetrahedron Lett. , 31 : 4985
  • Polt , R. and Peterson , M. A. Manuscript in preparation
  • Seyferth , D. 1962 . Prog. Inorg. Chem. , 3 : 129
  • Schöllkopf , U. 1970 . Houben-Weyl , Edited by: Müller , E. Vol. Band XIII/1 , 143 – 145 . Stuttgart : Georg Thieme Verlag . 159–160
  • Neumann , H. and Seebach , D. 1978 . Chem. Ber. , 111 : 2785 See refs. 3–7 therein for a concise review of alkenyllithium methodology
  • Jones , R. G. and Gilman , H. 1951 . Org. React. , 6 : 339
  • Kluge , A. F. , Untch , K. G. and Fried , J. H. 1972 . J. Am. Chem. Soc. , 94 : 7827 Here the substrate contains an ether linkage which promotes Li-l exchange
  • Corey , E. J. and Beames , D. J. 1972 . J. Am. Chem. Soc. , 94 : 7210
  • Cahiez , G. , Bernard , D. and Normant , J. F. 1976 . Synthesis , : 245
  • Zweifel , G. and Whitney , C. C. 1967 . J. Am. Chem. Soc. , 89 : 2753
  • 250 MHz 1H-nmr data for 4 : δ 5.76 ppm (dt, 1H, J = 6.2, 17 Hz), 4.92 ppm (d, 1H, J = 17 Hz), 2.05–1.95 ppm (m, 2H), 1.25 ppm (broad s, 22H), 0.88 ppm (t, 3H, J = 6.5 Hz)

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