References
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- Vallée , Y. , Masson , S. and Ripoll , J. L. 1990 . Tetrahedron , 46 : 3921 4c: The synthesis of 4a 4b has been previously described: yield = 20%. mp 82–83°C. 1H NMR (CDCl3): 1.13 (d, J = 7, 3H), 2.64 (dq, J = 7 and 2, 1H), 4.44 (d, J = 2, 1H), 5,61 (s, 1H), 7.0–7.4 (m, 8H). 13C NMR (CDCl3): 22.4, 52.9, 55.0, 74.0, 123.6–142.9 (12 aromatic C), 256.9 ppm. M. S.: 250 (M+., 11%), 178 (anthracene+., 100%). Anal. calc. for C17H14S: S 12.80, found S 12.75
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