References
- a search online in Chem. Abs. database indicated that 1 (mainly as 7-Oβ-D-glucoside) is reported more than 60 times for the period covered by issues 66 to 117. Among these references some are dealing with various ailments
- Bohlmann , F. , Zdero , C. and Kapteyn , H. 1968 . Lieb. Ann. Chemie , 717 : 168 see for exemple
- Caglioti , L. , Naef , H. , Arigoni , D. and Jeger , O. 1958 . Helv. Chim. Acta , 41 : 2278
- Hofer , O. and Greger , H. 1984 . Phytochem. , 23 ( 1 ) : 181
- Späth and Dobrovolny . 1938 . Chem. Ber. , 71 : 1831
- Ahluwalia , V. K. , Gupta , V. N. , Rustagi , C. L. and Seshadri , T. R. 1960 . J. Sci. Indus. Research , 19 ( B ) : 345
- Gorecki , P. and Mscisz , A. 1988 . Herba Pol. , 34 ( 1–2 ) : 43
- Aziz , M. and Rouessac , F. 1988 . Tetrahedron , 44 ( 1 ) : 101
- 1987 . Tetra. Letters , 28 ( 23 ) : 2579
- 1988 . Bull. Soc. Chim. Fr. , : 555
- Dean , F. M. 1963 . “Naturally Occuring Oxygen Compounds” , 176 London : Butterworths . Among the great number of different approaches to coumarins that have appeared in the literature the described methodology employing common intermediates transgresses the preparation of the sole fraxidin; It has been applied in our hands to other coumarins
- Adams , R. and Mathieu , J. 1948 . J. Amer. Chem. Soc. , 70 : 2120 This decarboxylation could be also accomplish by means of 25 % aqueous sodium bisulfite, see
- Kavanagh , K. R. and Pepper , J. M. 1954 . Can. J. Chem. , 32 : 216
- Iwasaki , T. and Takashima , K. Jpn Kokai Tokkyo Koho JP 03,157,351 [91,157,351] . in our hands, 5 NMR 1H (90 MHz) CDCl3, ppm: 4.02 (s, 6H, 2 MeO), 7.43 (s, H(6)), 10.45 (s, H(ald)). Mass Spectrum (m/z, rel. intensity): 262 (99); 261 (69); 260 (100) P+; 259 (39); 110 (11); 95 (13); 77 (11); 53 (11); 28 (23)
- Seidenfaden , W. and Pawellek , D. 1971 . “Methoden der Organische Chemie” , Vol. 10–1 , 863 Stuttgart : Houben-Weyl, Georg Thieme Verlag . see for exemple
- Russel , A. and Tebbens , W. G. Org. Syntheses , 22 35
- 1955 . Coll. , Vol. III : 293
- Keegstra , M. A. , Peters , T. H. A. and Brandsma , L. 1992 . Tetrahedron , 48 ( 17 ) : 3633
- Paradisi , C. 1991 . “Arene Substitution via Nucleophilic Addition to Electron Deficient Arenes” , Oxford : Pergamon Press . for a recent book on SNAr reactions, see Comprehensive Organic Synthesis Chapter 1
- Davidson , D. and Bernhard , S. A. 1948 . J. Amer. Chem. Soc. , 70 : 3426 purchased from Aldrich Co. or prepared according to
- zinc oxide 99.5 %, purchased to Janssen Chimica