Publication Cover
Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 23, 1993 - Issue 15
98
Views
4
CrossRef citations to date
0
Altmetric
Original Articles

A Convenient Preparation of (±)-α-Methoxy-α-trifluoromethylphenylacetic Acid (Mosher's Acid)

&
Pages 2145-2150 | Received 04 Mar 1993, Published online: 23 Sep 2006

References

  • Dull , D. L. and Mosher , H. S. 1967 . J. Am. Chem. Soc. , 89 : 4230
  • Dale , J. H. , Dull , D. L. and Mosher , H. S. 1969 . J. Org. Chem. , 34 : 2543
  • Yamaguchi , S. 1984 . “Asymmetric Synthesis” , Edited by: Morrison , J. D. Vol. 1 , New York : Academic Press . chapter 7
  • Parker , D. 1991 . Chem. Rev. , 91 : 1441
  • Hall , W. E. , Seeholzer , K. , Baumeister , M. and Ugi , I. 1986 . Tetrahedron , 42 : 547
  • Goldberg , Y. and Alper , H. 1992 . J. Org. Chem. , 57 : 3731 Very recently an alternative preparation involving addition of Cl3CCOOSiMe3 to 2 followed by hydrolysis was published:
  • Larock , R. C. 1989 . “Comprehensive Organic Transformations,” , 828 – 829 . New York : VCH . See, for example:
  • Lemieux , R. U. and vonRudloff , E. 1955 . Can. J. Chem. , 33 : 1701
  • Wolfe , S. , Hasan , S. K. and Campbell , J. R. 1970 . J. Chem. Soc., Chem. Commun. , : 1420
  • Carlsen , P. H. J. , Katsuki , T. , Martin , V. S. and Sharpless , K. B. 1981 . J. Org. Chem. , 46 : 3936
  • Sala , T. and Sargent , M. V. 1978 . J. Chem. Soc., Chem. Commun. , : 253
  • Patel , D. V. , VanMiddlesworth , F. , Donaubauer , J. , Gannett , P. and Sih , C. J. 1986 . J. Am. Chem. Soc. , 108 : 4603
  • Gassman , P. G. , Ray , J. A. , Wenthold , P. G. and Mickelson , J. W. 1991 . J. Org. Chem. , 56 : 5143
  • Brown , C. A. and Barton , D. 1974 . Synthesis , : 434
  • Hudlicky , M. 1990 . “Oxidations in Organic Chemistry,” , 273 Washington : American Chemical Society . Jones reagent was prepared by mixing 133.5 g of CrO3 in 200 mL of water, adding 115 mL of 98% H2SO4 with cooling, and diluting to a total volume of 500 mL with water:
  • Bowers , A. , Halsall , T. G. , Jones , E. R. H. and Lemin , A. J. 1953 . J. Chem. Soc. , : 2548
  • 1993–94 . Fluka Chemika-Biochemika catalogue, product #65371

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.