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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 24, 1994 - Issue 8
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Original Articles

Efficient Synthesis of Bromo- and Iodomethyltributyltin

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Pages 1117-1120 | Received 20 Sep 1993, Published online: 23 Sep 2006

References

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  • Saavedra , J. E. 1987 . “ Umpoled Synthons ” . Edited by: Hase , T. A. pp. 121 – 124 . New York : Wiley .
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  • Seitz , D. E. , Carroll , J. J. , Cartaya , M. C. P. , Lee , S.-H. and Zapata , A. 1983 . Synth. Commun. , 13 : 129
  • For a preparation of chloromethyltributyltin starting from tributyltin hydride that bears some resemblance to our procedure, see ref. 3c. The preparation of bromomethyltributyltin has, to our knowledge, not been described previously
  • Danheiser , R. L. , Romines , K. R. , Koyama , H. , Gee , S. K. , Johnson , C. R. and Medich , J. R. 1992 . Org. Synth. , 71 : 133
  • Kocienski , P. J. , Cernigliaro , G. and Feldstein , G. 1977 . J. Org. Chem. , 42 : 353
  • Bose , A. K. and Lal , B. 1973 . Tetrahedron Lett. , : 3937
  • Åhman , J. and Somfai , P. 1992 . Tetrahedron , 48 : 9537 For general experimental details, see
  • All glassware was washed with an ethanolic potassium hydroxide solution and then dried at 160 °C overnight prior to use

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