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- Excess E-3,5-iodohexadiene (2.5 equivalents) is required to force the alkylation to completion
- We thank Professor Les Hull (Union College) for recording the FT-IR of 4 for us
- We thank Mr. Rich Milberg of the Mass Spectrometry Laboratory at the University of Illinois at Urbana-Champaign for conducting the HRMS analysis of TIMDA adduct 4