Preparation of Diallyl Ketals

References

• Croxall , W. J. , Glavis , F. J. and Neher , H. T. 1948 . J. Am. Chem. Soc. , 70 : 2805
   Google Scholar
• Hirsh , D. H. , Hoaglin , R. J. and Kubler , D. G. 1958 . J. Org. Chem. , 23 : 1083
   Google Scholar
• Burkhardt , H. and Hausen , J. 1924 . Chem. Ber. , 57B : 795
   Google Scholar
• Lorette , N. B. and Howard , W. L. 1960 . J. Org. Chem. , 25 : 521
   Web of Science ®Google Scholar
• Howard , W. L. and Lorette , N. B. Org. Syn., Coll. , Vol. 5 292
   Google Scholar
• Sheppherd , W. A. and Bourns , A. N. 1956 . Can. J. Chem. , 34 : 123
   Google Scholar
• House , H. O. and Kramar , V. 1963 . J. Org. Chem. , 28 : 3362
   Google Scholar
• Ho , T-S. and Wong , C. M. 1975 . Syn. Comm. , 5 : 213
   Web of Science ®Google Scholar
• Ireland , R. E. , Norbeck , D. W. , Mandel , G. S. and Mandel , N. S. 1985 . J. Am. Chem. Soc. , 107 : 3285
   Web of Science ®Google Scholar
• Seitz , D. E. and Ferreira , L. 1979 . Syn. Comm. , 9 : 931
   Web of Science ®Google Scholar
• Beilstein , F. and Wiegand , E. 1885 . Ber. , 18 : 482 We prepared triallylorthoformate (bp760 195–205[ddot] C) by transesterification of trimethylorthoformate
   Google Scholar
• Tsunodu , T. , Suzuki , M. and Noyori , R. 1980 . Tetrahedron Lett. , 21 : 1357
   Google Scholar
• Mori , K. , Yoshimura , T. and Sugai , T. 1988 . Ann. , : 899
   Google Scholar
• D'Andrea , S. V. , Freeman , J. P. and Szmuszkovicz , J. 1991 . Org. Prep. Proc. Int. , 23 : 432
   Web of Science ®Google Scholar
• Rigby , J. H. and Senanayake , C. 1987 . J. Am. Chem. Soc. , 109 : 3147
   Google Scholar
• Ortholand , J. Y. and Greiner , A. 1993 . Bull. Soc. Chim. Fr. , 130 : 133
   Google Scholar
• Bleasedale , D. A. and Jones , D. W. 1991 . J. Chem. Soc. Perk. Trans. , I : 1683
   Google Scholar
• Heckman , B. , Mioskowski , J. Y. and Falck , J. R. 1992 . Tetrahedron Lett. , 33 : 5201
   Google Scholar
• Lillie , B. M. and Avery , M. A. 1994 . Tetrahedron Lett. , 35 : 969
   Web of Science ®Google Scholar
• The temperatures of the reactions were varied from -78[ddot] C to 0[ddot] C. Excess allyloxytrimethylsilane (4–6 equivalents) can be used to assure complete conversion. If the reaction appears to have stopped short of complete conversion, additional aliquots of TMSOTf can be added.
   Google Scholar