References
- 1992 1993 . NSF-REU participant
- Undergraduate research participant.
- Nahm , S. and Weinreb , S. M. 1981 . Tetrahedron Lett. , 22 : 3815
- Sibi , M. P. 1993 . Org. Prep. Proced. Int. , 23 : 15 For a review on the applications of N-methoxy-N-methylamides in synthesis see
- See Reference 3b
- Angelastro , M. R. , Peet , N. P. and Bey , P. 1989 . J. Org. Chem. , 54 : 3913 Reference 3b.(b)
- Angelastro , M. R. , Mehdi , S. , Burkhart , J. P. , Peet , N. P. and Bey , P. 1990 . J. Med. Chem. , 33 : 11
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- Irako , N. , Hamada , Y. and Shioiri , T. 1992 . Tetrahedron , 48 : 7251
- Brenner-Weiß , G. , Giannis , A. and Sandhoff , K. 1992 . Tetrahedron , 48 : 5855
- Davies , D. T. and O'Hanlon , P. J. 1988 . Synth. Commun. , 18 : 2273
- Braun , M. and Waldmüller , D. 1989 . Synthesis , : 856
- Angelastro , M. R. , Burkhart , J. P. , Bey , P. and Peet , N. P. 1992 . Tetrahedron Lett. , 33 : 3265
- Poss , M. A. and Reid , J. A. 1992 . Tetrahedron Lett. , 33 : 1411
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- Maugras , I. , Poncet , J. and Jouin , P. 1990 . Tetrahedron , 46 : 2807
- Einhorn , J. , Einhorn , C. and Luche , J-L . 1990 . Synth. Commun. , 20 : 1105
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- The reaction was performed at room temperature. Reaction at reflux gave higher yield (79%) but with lower optical purity (90%ee)
- The optical purity was determined by comparison of literature rotation values with those prepared in this study and by chiral HPLC analysis (see experimental section for details)
- Martinez , J. , Bali , J-P. , Rodriguez , M. , Castro , B. , Magous , B. , Laur , J. and Lignon , M-F . 1985 . J. Med. Chem. , 28 : 1874
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- Jurczak , J. and Golebiowski , A. 1989 . Chem. Rev. , 89 : 149 For leading references on the preparation of aldehydes from N-methoxy-N-methylamides see reference 2. For reviews on the chemistry of α-amino aldehydes see
- Fisher , L. E. and Muchowski , J. M. 1990 . Org. Prep. Proced. Int. , 22 : 399
- Roux , F. , Maugras , I. , Poncet , J. and Jouin , G. L. 1994 . Tetrahedron , 50 : 5345
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