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- NMR spectra were recorded at 300 MHz with Varian XL - 300 and in CDCl3 using TMS as internal standard, J values are given in Hz. Mass spectra were recorded with Shimadzu MS-QP 1000 spectrometer at 70ev. IR spectra were recorded with a Perkin - Elmer 681 spectrometer. The microanalysis was done on Carlo Erba strumentazione 1106 elemental analyser