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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 26, 1996 - Issue 1
129
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Original Articles

One Pot Synthesis of Oxazolidinones by Tosylation or Mesylation of N-Boc-β-Amino Alcohols

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Pages 83-88 | Received 09 May 1995, Published online: 21 Aug 2006

References and Notes

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  • Anderson , G. W. and Mcgregor , A. C. 1957 . J. Am. Chem. Soc. , 79 : 6180
  • Carpino , L. A. 1957 . J. Am. Chem. Soc. , 79 : 4427
  • Green , T. W. 1981 . Protective Groups in Organic Synthesis , 1st Ed. , 232 – 33 . New York : John Wiley and Sons .
  • Geiger , K. and Konig , W. 1981 . “ Amine Protecting Groups ” . In In The Peptides , Edited by: Gross , E. and Meienhofer , J. Volume 3 , 31 – 32 . New York : Academic Press .
  • Lee , J. W. , Son , H. J. , Lee , K. S. , Park , M. H. and Kim , B. O. 1994 . Kor. J. Med. Chem. , 4 : 126
  • Spectroscopic data of 3: 1H NMR (80 MHz, CDCl3) δ 1.46(s, 9H), 2.17(s, 3H), 3.22∼3.49(m, 3H), 3.57∼3.72(m, 3H), 3.77∼3.86(m, 1H), 4.16∼4.47(m, 3H); MS, m/e(relative intensity) 303(M+, 3.5), 247(35.2), 203(23.3), 126(29.2), 112(30.2), 88(49.6), 68(100), 57(78.1).
  • Curran , T. P. , Pollastri , M. P. , Abelleira , S. M. , Messier , R. J. , McCollum , T. A. and Rowe , C. G. 1994 . Tetrahedron Lett. , 35 : 5409 cf. Loss of Boc protecting group under basic conditions, see:
  • Agami , C. , Couty , F. , Hamon , L. and Venier , O. 1993 . Tetrahedron Lett. , 34 : 4509
  • Huwe , C. M. and Blechert , S. 1994 . Tetrahedron Lett. , 35 : 9533
  • Delaunay , D. and Le Corre , M. 1994 . J. Chem. Soc. Perkin Trans. 1 , 20 : 3041
  • Ishizuka , T. and Kunieda , T. 1987 . Tetrahedron Lett. , 28 : 4509

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