A Convenient Large Scale Synthesis of O-Benzylhydroxylamine

REFERENCES AND NOTES

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• The crude product can be easily purified with high yield (95%) by filtration of a dichloromethane solution through a pad of silica gel. Alternatively, crystallization with ethanol gave, with a 85% yield, a pure product having m.p. = 143–145°C.
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• With a longer reaction time (4 hours) the yield remained almost unaffected.
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