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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 27, 1997 - Issue 15
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Original Articles

A Mild and Convenient Deprotection of 4-Phenyl 1,3-Dioxolane Derivatives Under Catalytic Hydrogenation

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Pages 2691-2694 | Received 04 Feb 1997, Published online: 22 Aug 2006

References and notes

  • Greene , T. W. 1980 . Protective groups in organic synthesis , John Wiley & Sons, Inc. .
  • Corey , E. J. and Ruden , R. A. 1973 . J. Org. Chem. , 38 : 832
  • Katritzky , A. R. , Fan , W. Q. and Li , Q. L. 1987 . Tetrahedron Lett. , 28 : 1195
  • Zufan , Wu. , Mootoo , D. R. and Fraser Reid , B. 1988 . Tetrahedron Lett. , 29 : 6549
  • Lillie , B. M. and Avery , M. A. 1994 . Tetrahedron Lett. , 35 : 969
  • Masui , M. , Kawaguchi , T. and Ozaki , S. 1985 . JCS Chem. Comm. , : 1484
  • 2,4-benzodioxepines are known to be cleaved under catalytic hydrogenation, however, the present methodology offers advantages in preparation of chiral diols from styrene by asymetric dihydroxylation for a possible kinetic resolution of prochiral aldehydes.
  • Machinaga , N. and Kibayashi , C. 1989 . Tetrahedron Lett. , 30 : 4165
  • All products were characterised by comparing with standard sample.

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