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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 15
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Original Articles

Efficient One-Pot Synthesis of Jm3100

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Pages 2903-2906 | Received 06 Mar 1998, Published online: 20 Aug 2006

REFERENCES

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  • Bridger , G. J. , Skerlj , R. T. , Thornton , D. , Sreenivasan , P. , Martellicci , S. A. , Henson , G. W. , Abrams , M. J. , Yamamoto , N. , De Vreese , K. , Pauwels , R. and De Clerq , E. 1995 . J. Med. Chem. , 38 : 366
  • Esté , J. A. , De Vreese , K. , Witrouw , M. , Schmit , J.-C. , Vandamme , A.-M. , Anné , J. , Desmyter , J. , Henson , G. W. , Bridger , G. and De Clercq , E. 1996 . Antiviral Res. , 29 : 297
  • Brandes , S. , Gros , C. , Denat , F. , Pullumbi , P. and Guillard , R. 1996 . Bull. Soc. Chim. Fr. , 133 : 65
  • Gardinier , I. , Roignant , A. , Oget , N. , Bernard , H. , Yaouanc , J. J. and Handel , H. 1996 . Tetrahedron Lett. , 37 : 7711 and references cited herein
  • Use of chloroform was found to be necessary and its replacement by methylene chloride led to 1a in low yield (10–18%)
  • Filali , A. , Yaouanc , J.-J. and Handel , H. 1991 . Angew. Chem. Int. Ed. Engl. , 30 : 560
  • Spectral data for 1 and 3 were in agreement with reported data.2,9la: 13C NMR (D2O, 75 MHz) δ: 17.1, 17.9, 36.2, 40.2, 40.8, 42.6, 45.9, 57.1, 129.0, 131.6. 1b: 13C NMR (D2O, 75 MHz) δ: 43.1, 43.2, 45.1, 48.6, 57.1, 132.2, 136,1. 3a: 13C NMR (CDCl3. 75 MHz) δ: 21.5, 27.7, 41.3, 41.8, 43.8, 44.4, 45.4, 45.8, 51.2. 3b: 13C NMR (CDCl3, 75 MHz) δ: 43.6, 43.5
  • Richman , J. E. and Kubale , J. J. 1983 . J. Am. Chem. Soc. , 105 : 749

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