Regioselective Synthesis of New Triheterocyclic Compounds from 1,4-Benzodiazepine

References

• Hasnaoui , A. , El Messaoudi , M. and Lavergne , J.-P. 1985 . Recl. Trav. Chim. Pays-Bas , 104 : 129
   Google Scholar
• El Messaoudi , M. , Hasnaoui , A. , El Mouhtadi , M. , Goupil , J.-M. and Lavergne , J.-P. 1988 . J. Heterocyclic Chem. , 25 : 453
   Google Scholar
• El Messaoudi , M. , Hasnaoui , A. , El Mouhtadi , M. and Lavergne , J.-P. 1992 . Bull. Soc. Chim. Belg. , 101 : 977
   Google Scholar
• Hasnaoui , A. , Baouid , A. and Lavergne , J.-P. 1991 . J. Heterocyclic Chem. , 28 : 453
   Google Scholar
• Baouid , A. , Benharref , A. , Hasnaoui , A. and Lavergne , J.-P. 1994 . Bull. Soc. Chim. Belg. , 103 : 743
   Google Scholar
• El Messaoudi , M. , Hasnaoui , A. and Lavergne , J.-P. 1994 . Synth. Commun. , 24 : 513
   Web of Science ®Google Scholar
• Baouid , A. , Hasnaoui , A. and Lavergne , J.-P. 1996 . Bull. Soc. Chim. Belg. , 105 : 339
   Google Scholar
• Benelbaghdadi , R. , Hasnaoui , A. and Lavergne , J.-P. 1997 . Bull. Soc. Chim. Belg. , 106 : 813
   Google Scholar
• Bellantuono , C. , Reggi , G. , Tognoni , G. and Garattini , S. 1980 . Drugs , 19 : 195
   PubMed Web of Science ®Google Scholar
• Bartsch , H. and Erker , T. 1988 . J. Heterocyclic Chem. , 25 : 1151
   Web of Science ®Google Scholar
• Crystal data for 3d . C27H25ClN4O3 chemical formula weight: 488.98 Experimental crystal description: cube, colourless, crystal size max: 0.45, crystal size mid: 0.30, crystal size min: 0.20. Symmetry cell setting: monoclinic symmetry space group name h-m: P 21/n. Cell length a: 16.21(5), cell length b: 9.24(5), cell length c: 16.60(5), cell angle alpha: 90.00(2), cell angle beta: 94.42(2), cell angle gamma: 90.00(2), cell volume: 2468(1), cell formula units z: 4. Diffraction radiation type: Mo-K/α, radiation wavelength: 0.71073 A°. Cell measurement temperature: 298°K. Data collection: diffraction measurement device: Enraf Nonius CAD-4. Experimental absorption correction type: none. Diffraction reflections number: 6730, reflections number total: 4145, reflections number observed: 2165. Refinement data: refine 1s structure factor coefficient: F. Refine 1s R factor observed: 0.061, refine 1s wR factor observed: 0.052, refine 1s number reflections: 2165, refine 1s number parameters: 316. Atom type scattering source: International Tables for Xray Crystallography (1974 vol. 4).
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• Crystal data for 5d . C23H17ClN4O4 chemical formula weight: 448.87. Experimental crystal description: prism, colourless, crystal size max: 0.40, crystal size mid: 0.30, crystal size min: 0.20. Symmetry cell setting: monoclinic symmetry space group name h-m: P 21/n. Cell length a: 8.238(2), cell length b: 13.581(3), cell length c: 18.540(3), cell angle alpha: 90.00(1), cell angle beta: 94.42(1), cell angle gamma: 90.00(1), cell volume: 2068(1), cell formula units z: 4. Diffraction radiation type: Mo-K/α, radiation wavelength: 0.71073 A°. Cell measurement temperature: 294°K. Data collection: diffraction measurement device: Enraf Nonius CAD-4. Experimental absorption correction type: none. Diffractionn reflections number: 7513, reflections number total: 3632, reflections number observed: 2562. Refinement data: refine 1s structure factor coefficient: F. Refine 1s R factor observed: 0.058, refine 1s wR factor observed: 0.045, refine 1s number reflections: 2562, refine 1s number parameters: 290. Atom type scattering source: International Tables for Xray Crystallography (1974 vol.4).
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