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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 22
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Original Articles

Beckmann Fragmentation of Diphenylcarbamoylated N-Aryldiphenacylamine Dioximes. New Method for the Synthesis of Imidazooxadiazolones

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Pages 3889-3894 | Accepted 17 Mar 1999, Published online: 17 Sep 2007

References

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  • To prove the structure of the diphenacylamine dioximes we have prepared 3c starting from phenacylaniline which was first converted to diphenacylaniline reacting with phenacyl bromide.The reaction of diphenacyhiline with hydroxylamine hydrochloride in the presence of sodium acetate afforded a compound identical to those obtained via the reaction of aniline with phenacyl bromide oxime. IR, 1H NMR and elemental analysis data confirmed the assigned structure.
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