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- To prove the structure of the diphenacylamine dioximes we have prepared 3c starting from phenacylaniline which was first converted to diphenacylaniline reacting with phenacyl bromide.The reaction of diphenacyhiline with hydroxylamine hydrochloride in the presence of sodium acetate afforded a compound identical to those obtained via the reaction of aniline with phenacyl bromide oxime. IR, 1H NMR and elemental analysis data confirmed the assigned structure.
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