References
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- For all IR spectra: strong, vs very strong, m middle, w weak, vw very weak, br broad.
- In the IR spectra of compounds 3a, 9b, and 9c the bands of stretching vibration of a-OH groups shift below 3000 cm -1, become more broad and so they are difficult to observe
- IR and 1 H NMR spectra of compounds 8a-c were obtained using dry solvents
- In the IR and 1H NMR spectra of gem-diols 9a-c in CD Cl3 and CDCl3 the proton signals of corresponding oxo derivatives 8a-c were observed
- Owing to relative lability the sharp melting points and satisfactory elemental analysis of gem-diols 9a-c were not obtained