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Food Additives & Contaminants Volume 24, 2007 - Issue 11
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Original Articles

Validation of an analytical method for the determination of carbadox and olaquindox in feedstuff by liquid chromatography coupled to UV and/or diode array detection

G. Gizzi European Commission, Joint Research Centre, Institute for Reference Materials and Measurements, Food Safety and Quality Unit, Retieseweg, B-2440 Geel, Belgium
,
U. Vincent European Commission, Joint Research Centre, Institute for Reference Materials and Measurements, Food Safety and Quality Unit, Retieseweg, B-2440 Geel, Belgium
,
C. von Holst European Commission, Joint Research Centre, Institute for Reference Materials and Measurements, Food Safety and Quality Unit, Retieseweg, B-2440 Geel, BelgiumCorrespondence[email protected]
,
J. de Jong RIKILT Institute of Food Safety, Bornsesteeg 45, 6708 PD Wageningen, The Netherlands, P. O. Box 230
&
C. Genouel Laboratoire de la Direction Générale de la Concurrence, de la Consommation et de la Répression des Fraudes (L35-DGCCRF), Rue Antoine Joly 26, F-35000 Rennes, France
Pages 1226-1235 | Received 23 Nov 2006, Accepted 18 Apr 2007, Published online: 09 Oct 2007

References

  • de Jong , J , Tomassen , MJH , van Egmond , HJ , van Rhijn , JA , Zuidema , T , Michard , J , Genouel , C , Brambilla , G , Nunes da Costa , JMG Nordkvist , E . 2006 . “ Towards a control strategy for banned antibiotics and growth promoters in feed: the SIMBAG-FEED project ” . In Antimicrobial growth promoters Where do we go from here? , Edited by: Barug , D , de Jong , J , Kies , AK and Verstegen , MWA . Wageningen : Wageningen Academic Publishers . ISBN: 90-7699887
  • European Communities . 1993 . Eleventh Commission Directive 93/70/EEC of 28 July 1993 establishing Community analysis methods for official control of feedstuffs . Official Journal of the European Communities , L 234 : 17 – 21 .
  • European Communities . 1998a . Council Regulation No 2821/98 of 17 December 1998 amending, as regards withdrawal of the authorisation of certain antibiotics, Directive 70/524/EEC concerning additives in feedstuffs . Official Journal of the European Communities , L 351 : 4 – 8 .
  • European Communities . 1998b . Commission Regulation (EC) No 2788/98 of 22 December 1998 amending Council Directive 70/524/EEC concerning additives in feedstuffs as regards the withdrawal of authorisation for certain growth promoters . Official Journal of the European Communities , L 347 : 31 – 32 .
  • European Communities . 1998c . Commission Directive 98/64 of 3 September 1998 establishing Community methods of analysis for the determination of amino acids, crude oils and fats, and olaquindox in feedstuffs and amending Directive 71/393/EEC . Official Journal of the European Communities , L 257 : 14 – 46 .
  • European Communities . 1999 . Commission Directive 1999/27/EC of 20 September 1999 establishing Community methods of analysis for the determination of amprolium, diclazuril and carbadox in feedstuffs and amending Directive 71/250/EEC, 73/46/EEC and repealing Directive 74/203/EEC . Official Journal of the European Communities , L 118 : 36 – 52 .
  • European Communities . 2002 . Commission Decision 2002/657/EC of 12 August 2002 implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results . Official Journal of the European Communities , L 221 : 8 – 36 .
  • Genouel , C . 2004 . Final method description. Animal feedstuffs. Simultaneous determination of carbadox and olaquindox content. Method using HPLC. SIMBAG-FEED report on Deliverable 5.6. Available from IRMM and RIKILT at http://www.rikilt.wur.nl/NR/rdonlyres/23469735-C6B5-4F61-9097-06BBCB3D0D8A/30269/SIMBAGFEEDMethodHPLCCARBndOLA.pdf. Accessed 23 November 2006
  • Genouel , C . 2005 . Refined method description. Animal feedstuffs. Simultaneous determination of carbadox and olaquindox content. Method using HPLC. SIMBAG-FEED report. Available from IRMM and RIKILT at http://www.rikilt.wur.nl/NR/rdonlyres/23469735-C6B5-4F61-9097-06BBCB3D0D8A/30269/SIMBAGFEEDMethodHPLCCARBandOLA.pdf. Accessed 23 November 2006
  • Horwitz , W , Kamps , LR and Boyer , KW . 1980 . Quality assurance in the analysis of foods and trace constituents . Journal of the Association of Official Analytical Chemistry , 63 : 1344 – 1354 .
  • Horwitz , W . 1995 . Protocol for the design, conduct and interpretation of method-performance studies . Pure and Applied Chemistry , 67 : 331 – 343 .
  • Horwitz , W and Albert , R . 2006 . The Horwitz ratio (HORRAT): A useful index of method performance with respect to precision . Journal of AOAC International , 89 : 1095 – 1109 .
  • Kramer , GN , Oostra , A , de Vos , P , Teipel , K , Emteborg , H and Conneely . 2004 . Production of fourblank and 10 spiked compound feeds for SCA SIMBAG-FEED. SIMBAG-FEED report 8.5, GER/RM/10/2004/November/10 Available from IRMM and RIKILT at http://www.rikilt.wur.nl/NR/rdonlyres/23469735-C6B5-4F61-9097-06BBCB3D0D8A/30269/SIMBAGFEEDMethodHPLCCARBandOLA.pdf Accessed 23 November 2006
  • Thomspson , M and Wood , R . 1993 . The International Harmonised Protocol for the proficiency testing of (chemical) analytical laboratories . Pure and Applied Chemistry , 65 : 2123 – 2144 .
  • Vincent U, Gizzi G, von Holst C, de Jong J, Michard J. 2007. Validation of an analytical method for the determination of spiramycin, virginiamycin and tylosin in feedstuffs by thin layer chromatography and bioautography. Food Additives & Contaminants 24:351–359

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