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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 19
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Original Articles

PREPARATION OF TRIBUTYLBORANE FROM BUTYLLITHIUM AND BORON TRIFLUORIDE ETHERATE

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Pages 2939-2942 | Received 19 Sep 2000, Published online: 16 Aug 2006

REFERENCES

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  • Ref. [6a]
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  • Suffert , J. 1989 . For an accurate stoichiometry, it is recommended to titrate the commercially available n-butyllithium before use. Suffert's method for instance, is quite convenient and gives satisfactory results . J. Org. Chem. , 54 : 509 – 510 .

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