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- Starting material 1 was commercially available from Acros Organics in New Jersey USA
- The crystal of compound 3a belongs to the triclinic system, space group PI with parameters: a = 8.398(1), b = 10.206(1), c = 14.538(2) Å, α = 75.221(3)°, β = 85.965(3)°, γ = 81.746(3)°, V = 1191.6(3) Å3, S = 1.028, Z = 4, Dc = 1.378 Mg/m3, μ = 0.233 mm−1, F(000) = 520, λ (MoKa) = 0.71073 Å, T = 293(2) K, final R = 0.071 and wR = 0.1953 for 4177 independent reflections with I≥2σ(I)
- The crystal of compound 9 belongs to the monoclinic system, space group C2/c with parameters: a = 17.8408(18), b = 8.3725(9), c = 16.7401(18) Å, β = 118.997(2)°, V = 2187.0(4) Å3, Z = 8, Dcalc = 1.374 Mg/m3, μ = 0.240 mm−1, F(000) = 944, λ (MoKa) = 0.71073 Å, T = 293(2) K. The final R and wR are 0.0499 and 0.1436 respectively for 2240 independent reflections with I≥2σ(I)