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Materials Research Innovations Volume 2, 1999 - Issue 6
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Original Article

Structure of low temperature phase γ-LaSc3(BO3)4 crystal

Guofu WangFujian Institute of Research on the Structure of Matter, Chinese Academy of Science, Fuzhou, Fujian350002, P.R. China Fax: +0086-591-3714946, e-mail: [email protected]
,
Meiyun HeFujian Institute of Research on the Structure of Matter, Chinese Academy of Science, Fuzhou, Fujian350002, P.R. China Fax: +0086-591-3714946, e-mail: [email protected]
,
Wenzhi ChenFujian Institute of Research on the Structure of Matter, Chinese Academy of Science, Fuzhou, Fujian350002, P.R. China Fax: +0086-591-3714946, e-mail: [email protected]
,
Zhoubin LinFujian Institute of Research on the Structure of Matter, Chinese Academy of Science, Fuzhou, Fujian350002, P.R. China Fax: +0086-591-3714946, e-mail: [email protected]
,
Shaofang LuFujian Institute of Research on the Structure of Matter, Chinese Academy of Science, Fuzhou, Fujian350002, P.R. China Fax: +0086-591-3714946, e-mail: [email protected]
&
Qiangjin WuFujian Institute of Research on the Structure of Matter, Chinese Academy of Science, Fuzhou, Fujian350002, P.R. China Fax: +0086-591-3714946, e-mail: [email protected]
Pages 341-344 | Received 27 Oct 1998, Accepted 12 Nov 1998, Published online: 13 Oct 2016
 
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Abstract

We reported the investigating results of the phase transition and phase structure for LaSc3(BO3)4 crystal. LaSc3(BO3)4 crystal exist three phases: high temperature phase a-LaSc3(BO3)4 with space group C2/c, medium temperature phase β-LaSc3(BO3)4 with space group R32 and low temperature phase γ -LaSc3(BO3)4 with space group Cc. Title compound γ -LaSc3(BO3)4 crystallizes in the monoclinic with space group Cc, and the unit cell dimensions, a=7.740(3) Å, b=9.864(2) Å, c=12.066(5) Å, β =105.48(5)°C, V=887.8(6) Å3, Z=4, DC=3.81 g/cm3, λ (MoKα)=0.71067 Å, F(000)=944, final R=0.040, RW=0.054 for 1840 observed reflection with I≥3σ>(I).

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