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Analytical Letters Volume 5, 1972 - Issue 5
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Original Articles

The Reactions of SO3 and SbF5 with Fluorosulfuric Acid

J. Badoz-lambling Laboratoire de Chimie, Analytique associe au C. N. R. S., 10 rue Vauquelin. 75, Paris, VO, France
,
M. Herlem Laboratoire de Chimie, Analytique associe au C. N. R. S., 10 rue Vauquelin. 75, Paris, VO, France
,
A. Thiebault Laboratoire de Chimie, Analytique associe au C. N. R. S., 10 rue Vauquelin. 75, Paris, VO, France
&
G. Adhami Laboratoire de Chimie, Analytique associe au C. N. R. S., 10 rue Vauquelin. 75, Paris, VO, France
Pages 305-308 | Received 04 Apr 1972, Accepted 25 Apr 1972, Published online: 06 Dec 2006
 
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Abstract

Fluorosulfuric acid is a good donor of SO3 and as a result it reacts with SbF5 to give HSbF6 and SO3. Solutions of SO3 and SbF5 in fluorosulfuric acid exhibit the same cathodic waves at platinum and platinized platinum electrodes. Electrochemical reductions at a potential corresponding to the plateau of these waves produces SO2 and not H2.

We have investigated the reactions of SO3 and SbF5 with flurosulfuric acid.

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