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Analytical Letters Volume 5, 1972 - Issue 10
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ELECTROCHEMISTRY

Trace Analysis by ESCA-Electrochemical Measurements

J. S. Brinen American Cyanamid Company, Stamford, Connecticut, 06904
&
J. E. McClure American Cyanamid Company, Stamford, Connecticut, 06904
Pages 737-743 | Received 14 Sep 1972, Accepted 16 Sep 1972, Published online: 06 Dec 2006
 
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Abstract

A procedure which combines electrochemical deposition and ESCA measurements for the determination of trace levels of metals in solution is described. The method is demonstrated by an experiment in which microgram quantities of Pb, Cd, and Bi are deposited on a mercury-coated platinum electrode and then detected by ESCA measurements.

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