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Analytical Letters Volume 14, 1981 - Issue 3
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SPECTROMETRY

Fused Silica Capillary GC with Boron Specific Microwave Excited Plasma Detection in Derivatization and Polymer Pyrolysis

Louis G. Sarto Jr. Department of Chemistry, GRC Tower A, University of Massachusetts, Amherst, Mass, 01003
,
Scott A. Estes Department of Chemistry, GRC Tower A, University of Massachusetts, Amherst, Mass, 01003
,
Peter C. Uden Department of Chemistry, GRC Tower A, University of Massachusetts, Amherst, Mass, 01003
,
Sidney Siggia Department of Chemistry, GRC Tower A, University of Massachusetts, Amherst, Mass, 01003
&
Ramon M. Barnes Department of Chemistry, GRC Tower A, University of Massachusetts, Amherst, Mass, 01003
Pages 205-218 | Received 02 Jan 1981, Accepted 05 Jan 1981, Published online: 24 Feb 2007
 
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Abstract

Boron specific element detection for capillary column gas chromatography is achieved by atmospheric pressure microwave induced and sustained helium plasma spectroscopic emission. A small flow of hydrogen is added to the helium to enhance general plasma characteristics for boron emission. Fused silica capillary column applications are discussed for boronate derivatives of diols and in carborane silicone polymer pyrolysis.

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