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Analytical Letters Volume 19, 1986 - Issue 21-22
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Original Articles

Determination of Hydrogen in Zircaloy by Spark Source Mass Spectrometry

K. L. Ramakumar Fuel Chemistry Division, Bhabha Atomic Research Centre Trombay, Bombay, 400085, India
,
V. A. Raman Fuel Chemistry Division, Bhabha Atomic Research Centre Trombay, Bombay, 400085, India
,
V. L. Sant Fuel Chemistry Division, Bhabha Atomic Research Centre Trombay, Bombay, 400085, India
,
P. M. Shah Fuel Chemistry Division, Bhabha Atomic Research Centre Trombay, Bombay, 400085, India
,
V. D. Kavimandan Fuel Chemistry Division, Bhabha Atomic Research Centre Trombay, Bombay, 400085, India
&
H. C. Jain Fuel Chemistry Division, Bhabha Atomic Research Centre Trombay, Bombay, 400085, India
Pages 2147-2154 | Received 25 Aug 1986, Accepted 16 Sep 1986, Published online: 03 Jan 2007
 
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Abstract

Application of Spark Source Mass Spectrometry(SSMS) for the determination of hydrogen in zircaloy clad material used in nuclear reactors is reported. The advantage of SSMS lies in the fact that along with the metallic trace constituents even the nonmetallics including the gaseous impurities can also be determined in a single analysis using the photoplate detection system. The value obtained for H2 using photoplate detection system is compared with that obtained in electrical detection system in SSMS and also with the value obtained employing the conventional inert gas fusion technique.

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