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Analytical Letters Volume 20, 1987 - Issue 5
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SPECTROMETRY

Application of Xanthene Derivatives in Analytical Chemistry Part LXV. The Spectrophotometric Determination of Vanadium with O-Hydroxyhydroquinonephthalein in the Presence of Cationic Surfactants

Itsuo Mori Osaka University of Pharmaceutical Sciences, Matsubara, Osaka, 580, Japan
,
Yoshikadzu Fujita Osaka University of Pharmaceutical Sciences, Matsubara, Osaka, 580, Japan
,
Kinuko Fujita Osaka University of Pharmaceutical Sciences, Matsubara, Osaka, 580, Japan
,
Takeshi Tanaka Osaka University of Pharmaceutical Sciences, Matsubara, Osaka, 580, Japan
,
Yoshihiro Nakahashi Osaka University of Pharmaceutical Sciences, Matsubara, Osaka, 580, Japan
&
Ayumi Yoshii Osaka University of Pharmaceutical Sciences, Matsubara, Osaka, 580, Japan
Pages 747-760 | Received 20 Jan 1987, Accepted 13 Feb 1987, Published online: 06 Dec 2006
 
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Abstract

The colour reaction between o-hydroxyhydroquinonephthalein and vanadate ion in the presence of hexadecyltri-methylammonium chloride and L-ascorbic acid as a reductant was discussed. And the spectrophotometric determination of vanadium utilizing the colour reaction system in micellar media was proposed at about pH 5.4. Beer's law was obeyed in the concentration range 0-8 μg of vanadium at 540 nm. The apparent molar extinction was 8.7 × 10 4 1 mol−1 cm−1 with Sandell sensitivity of 0.0006 μg/cm2. This proposed method was relatively simple and sensitive, and then its applications for the waste water, river water, rain water, etc. were discussed.

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