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ENVIRONMENTAL ANALYSIS

A Microwave Digestion Method for Total Decomposition of Lead and Other Metals in Paint, Soil and Dust

Pages 3397-3406 | Received 18 May 2000, Accepted 09 Aug 2000, Published online: 01 Jun 2011
 

ABSTRACT

A simple, total decomposition method for lead and other metals in paint has been developed. Complete decomposition is achieved through a combination of reagents over several digestive steps in a microwave oven. Results of analysis of several NIST paint SRMs show excellent recoveries ranging from 85.5 to 111%. Additionally, recoveries of a number of trace elements for two soil and one dust NIST SRM were also excellent.

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