Neutron diffraction studies of Pb(Zr_xTi_1−x)O₃ ceramics

Johannes Frantti Materials and Structures Laboratory, Tokyo Institute of Technology, 4259 Nagatsuta, Midori-ku, Yokohama, 226-8503, Japan

Jyrki Lappalainen Microelectronics and Materials Physics Laboratories, University of Oulu, Linnanmaa P.O. Box 4500, FIN-90014, University of Oulu, Finland

Sten Eriksson Studsvik Neutron Research Laboratory, Uppsala University, S-61182, Nyköping, Sweden

Sergey Ivanov X-Ray Laboratory, Department of Inorganic Materials, Karpov Institute of Physical Chemistry, 103064, ul. Vorontsovo pole, 10, Moscow, Russia

Vilho Lantto Microelectronics and Materials Physics Laboratories, University of Oulu, Linnanmaa P.O. Box 4500, FIN-90014, University of Oulu, Finland

Shigeru Nishio Materials and Structures Laboratory, Tokyo Institute of Technology, 4259 Nagatsuta, Midori-ku, Yokohama, 226-8503, Japan

Masato Kakihana Materials and Structures Laboratory, Tokyo Institute of Technology, 4259 Nagatsuta, Midori-ku, Yokohama, 226-8503, Japan

Håkan Rundlöf Studsvik Neutron Research Laboratory, Uppsala University, S-61182, Nyköping, Sweden

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Abstract

The crystal structure of Pb(Zr_xTi_1−x)O₃ powders, 0.20≤x≤0.54, was determined using neutron diffraction measurements. At room temperature the structure was tetragonal (P4mm) for x≤0.50 and monoclinic (Cm) for 0.52≤x≤0.54. The sample having x=0.50 transformed from tetragonal symmetry to monoclinic at low temperature.

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Neutron diffraction studies of Pb(Zr_xTi_1−x)O₃ ceramics