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Research Article

Failure of epoxies bonded assemblies: comparison of thermal and humid ageing

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Pages 945-968 | Received 22 Aug 2018, Accepted 08 Nov 2018, Published online: 03 Dec 2018
 

ABSTRACT

This paper deals with the effect of Ti/epoxy/Ti bonded assemblies submitted either to wet (70°C, 85% HR) or thermal (120°C in oven) ageing. It was observed that humid ageing leads to an adhesive failure whereas thermal ageing leads to a cohesive one with the appearance of cracks at the edges of samples. The mechanical failures were shown to be mainly driven by the degradation of the epoxy adhesive. The thermal and water ageing of epoxy was thus studied and some relevant parameters (water diffusion coefficient for humid ageing, oxidation rate and thickness of oxidized layer for thermal ageing) were estimated so as to discuss on the predominance of thermal or humid ageing depending to the exposure conditions.

Acknowledgements

Agence Nationale de la Recherche et de la Technologie is gratefully acknowledged for having granted this study (Cifre N° 2015-0424)

Additional information

Funding

This work was supported by the Association Nationale de la Recherche et de la Technologie [2015-0424].

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