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Organic Preparations and Procedures International
The New Journal for Organic Synthesis
Volume 43, 2011 - Issue 4
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Original Articles

Simple and Efficient Method for the Synthesis of Azides in Water-THF Solvent System

M. Swetha Department of Chemistry, N. S. B. College, Vazirabad, Nanded, Maharashtra, India, - 431 601
,
P. Venkata Ramana Department of Chemistry, University College of Science, Osmania University, Hyderabad, Andhra Pradesh, India, - 500 007
&
S. G. Shirodkar Department of Chemistry, N. S. B. College, Vazirabad, Nanded, Maharashtra, India, - 431 601
Pages 348-353 | Received 31 Dec 2010, Accepted 05 May 2011, Published online: 02 Aug 2011
 
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Acknowledgement

Authors M. S. and P. V. R. acknowledge the Principal, N. S. B. College, Nanded and the Director, Central Facility Building for Research and Development, Osmania University, Hyderabad for providing spectral facilities.

Notes

aPurity based on GC analysis: column OV-1carrier gas flow H2/N2:18 mL/min. sample size 0.2 mL.

bPurity by GC after distillation.

cPurity based on GC-MS analysis: Isolated compound subjected to GC-MS by dissolving in DCM.

dMelting point.

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