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Liquid Cu–Pb alloys containing 14.7; 34.5; 40 and 67 at.% Pb were investigated by means of X–ray scattering method. Temperatures at which structure factors were measured are corresponding to one phase region on the phase diagram. Analysis of the structure factors and calculated pair correlation functions may possible to conclude that tendency to microsegregation is most pronounced at 34.5 and 40 at.% Pb.
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