Mass Spectral Studies of Biheteroaryls: Part 3. Identification of Dimeric Products Obtained from the Homolytic Methylation of the Lutidines

Kenneth C. Bass Department of Chemistry, The City University, London, EC1V OHB, England

Barry McIntosh Department of Chemistry, The City University, London, EC1V OHB, England

Alan G. Osborne Department of Chemistry, The City University, London, EC1V OHB, England

Abstract

The dimeric products formed during the homolytic methylation of the lutidines with t-butyl peroxide at 135° have been identified by gas chromatography — mass spectrometry. The 2,6- and 3,5- lutidines gave the corresponding dimethyldipyridylethanes whilst the 2,4-, 2,5- and 3,4- lutidines gave both the normal and crossed products.

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Mass Spectral Studies of Biheteroaryls: Part 3. Identification of Dimeric Products Obtained from the Homolytic Methylation of the Lutidines

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Mass Spectral Studies of Biheteroaryls: Part 3. Identification of Dimeric Products Obtained from the Homolytic Methylation of the Lutidines

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