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The electron spin resonance (ESR) of radicals obtained by electrolytic reduction of 4-[2-(3,4-Dimethoxiphenyl)ethyl]-1-(5-nitrofurfurylidine)semicarbazide and 4-[2-(3,4-Dimethoxyphenyl)ethyl]-1-(5-nitrothienilydene)semicarbazide were measured in DMSO. The electrochemistry of these compounds was studied in DMSO, DMF and ACN using cyclic voltammetry.
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